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c/coldchain·posted 2 years ago by u/india_generic_g

[Question] New Zealand — has anyone got a straight answer on lyophilised

Question Long Haul ×1

New Zealand — has anyone got a straight answer on lyophilised. I am not trying to be the "source?" guy. I would just like a source.

Ordered from the warehouse in Spain instead of origin and the transit went from a fortnight to 9 days. Entirely different proposition in August.

A transit temperature logger records a distribution, and time above a threshold matters as much as peak temperature. That is the argument for logging rather than guessing.

Regional stock changes the question rather than answering it: shorter lanes mean less exposure and fewer variables, which is why the warehouse question is worth asking before ordering in summer.

If two or three other people have done the same thing we might actually learn something. Alone it is an anecdote.

6,006 up / 5,244 down53% upvoted31 commentsid tq8sf211 Jul 2024

31 comments

28 in this archive, depth 4

best — the order this archive was captured in

u/curious_panel_only55 points·2 years ago

Lyophilisation removes the water that drives most degradation pathways. That is why the dry cake is comparatively robust and the reconstituted solution is not.

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u/gustav_vermeulen18 points·2 years ago

a summer lane and a winter lane are different lanes

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u/transit_variance5 points·2 years ago

Was there a logger in the box?

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u/coldchain_karenMOD42 points·2 years ago

Retitled: the original asserted degradation the post does not evidence.

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u/plain_titration_202433 points·2 years ago

Cosigning the regional stock point. Ordering from a warehouse in Ireland took the whole question off my table.

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u/bence_ibarra25 points·2 years ago

ask what storage condition the stability statement was written against

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u/cesar_teixeira8 points·2 years ago

How many days in transit, and which month?

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u/reship_roulette4 points·2 years ago

regional stock removes most of this problem entirely

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u/adaeze_weiss25 points·2 years ago

lyophilised powder is far more forgiving than the panic threads suggest

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u/mod_cold_roommod · c/coldchain21 points·2 years ago

Gel packs are designed for a duty cycle. A liquid pack at the end of a longer-than-expected transit is a pack behaving as specified, not evidence of an excursion in the vial.

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u/nightowl_injector16 points·2 years ago

if you want to know, log it, otherwise you are guessing

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u/kian_solberg13 points·2 years ago

insulation buys hours, not days

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u/india_generic_gOP7 points·2 years ago

transit temperature is a distribution, not a number

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[removed]9 points·2 years ago

[removed by moderator]

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u/marta_ilunga10 points·2 years ago

Once in solution, the relevant risks are hydrolysis, aggregation and, for some sequences, oxidation. Refrigeration slows all three; freezing a solution introduces a separate risk at the ice interface.

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u/india_generic_gOP8 points·2 years ago

Where in the fridge is it sitting now?

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u/rohan_steiner-18 points·2 years ago

You cannot infer potency from a temperature record. The record tells you what happened to the box; only a test tells you what happened to the material.

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u/plain_titration_202427 points·2 years ago

Split an order across two months deliberately to compare summer and winter transit on the same lane. Four days difference, same carrier.

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u/bruno_dumitru17 points·2 years ago

Split an order across two months deliberately to compare summer and winter transit on the same lane.

plain_titration_2024 is right that the pack failing is not the material failing. Two separate claims.

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u/certified_referenceQC17 points·2 years ago

Seasonality, which the source-page lane tables show clearly once you look for it.

The same origin, destination and carrier can differ by several days between February and August, and the temperature exposure differs by much more than the transit time suggests. A lane that is uneventful in winter is the same lane that generates the summer threads.

Two practical consequences. First, compare like months when you compare lanes. Second, ask which lines a supplier holds in regional stock — a shorter leg in July is worth more than any amount of packaging.

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u/low_appetite_lisa5 points·2 years ago

Agreed on seasonality. The same lane in February and August is not the same lane.

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u/niels_yilmaz9 points·2 years ago

Do you know what storage condition the stability statement covers?

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u/india_generic_gOP4 points·2 years ago

Moved everything off the fridge door after reading a thread here and my temperature log immediately got boring.

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u/iman_castellanos2 points·2 years ago

Correction: that stability figure covers the lyophilised powder, not the reconstituted solution. Different claim entirely.

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u/spain_receta4 points·2 years ago

powder at room temperature for a few days is usually a non-event

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u/maren_sorensen13 points·2 years ago

A stability statement is only meaningful with its conditions attached: temperature, duration, light exposure, and whether it covers powder or solution. Ask which.

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u/phase_two_pete6 points·2 years ago

This. A liquid gel pack on arrival tells you about the pack’s duty cycle, not about the vial.

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u/ireland_drugs_pay9 points·2 years ago

the excursion that matters is the one after reconstitution

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Temperature and stability in the real world: what an excursion actually costs you, why lyophilised powder is far more forgiving than reconstituted solution, how to read a logger CSV, and how to photograph a failed shipment so the conversation with the vendor is short.

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